@ARTICLE{Kwiatkowski_Kamil_High-temperature_2023,
 author={Kwiatkowski, Kamil and Piz, Mateusz and Filipek, Elżbieta},
 volume={vol. 44},
 number={No 4 (24th Polish Conference of Chemical and Process Engineering, 13-16 June 2023, Szczecin, Poland. Guest editor: Prof. Rafał Rakoczy)},
 journal={Chemical and Process Engineering: New Frontiers},
 pages={e44},
 howpublished={online},
 year={2023},
 publisher={Polish Academy of Sciences Committee of Chemical and Process Engineering},
 abstract={In the presented work, the conditions of the high-temperature and mechanochemical method for the synthesis of compound Sm 5VO 10 and their influence on its physicochemical properties were studied. The following methods were used for the study: X-ray powder diffraction (XRD), differential thermal analysis (DTA), infrared spectroscopy (FTIR), ultraviolet and visible light spectroscopy (UV–VIS–DRS), scanning electron microscopy (SEM-EDX), and laser beam diffraction spectrometry (LDS). Based on the results, it was determined that the compound Sm 5VO 10 is thermally stable in air atmospheres up to 1475 °C, crystallises in a monoclinic system, and its structure is made up of oxygen VO 4 and SmO 8 polyhedra. The estimated energy gap value for nanometric, mechanochemically obtained Sm 5VO 10 was about 3.20 eV, and for the microcrystalline, obtained with the high-temperature method, was about 2.75 eV. The established physicochemical characterisation of Sm 5VO 10 initially showed that the compound could find potential applications, e.g. as a photocatalyst for water purification or as a component of new optoelectronic materials.},
 type={Article},
 title={High-temperature and mechanochemical synthesis of Sm 5VO 10 and its unknown properties},
 URL={http://www.czasopisma.pan.pl/Content/129344/e44_int.pdf},
 doi={10.24425/cpe.2023.147403},
 keywords={high temperature and mechanochemical synthesis, Sm5VO10 compound, thermal stability, XRD, semiconductor},
}