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Abstract

The paper presents research results on the selection of parameters for the asymmetric rolling process of bimetallic plates 10CrMo9-10 + X2CrNiMo17-12-2. They consisted in determining the optimum parameters of the process, which would be ensured to obtain straight bands. Such deformation method introduces in the band the deformations resulting from shear stress, which affect changes in the microstructure. But their effect on the structure is more complicated than in the case of homogeneous materials. It has been shown that the introduction of asymmetric conditions into the rolling process results in greater grain refinement in the so-called hard layer. There was no negative effect on the structural changes in the soft layer observed.

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Authors and Affiliations

D. Rydz
ORCID: ORCID
B. Koczurkiewicz
G. Stradomski
T. Garstka
J. Wypart
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Abstract

The forming limit of AZ31 alloy, a representative Mg-Al-Zn-based wrought alloy, and the effect of severe plastic deformation (SPD) by examining the microstructure change caused by dynamic recrystallization led by high temperature and high dislocation density at 300℃ using a biaxial alternate forging (BAF) were investigated in this study. As a result of BAF test for AZ31 Mg alloy, significant cracks on the ends of workpieces occurred after 7 passes. The microstructure of as-extruded specimen showed the non-uniform distribution of the relatively coarse grains and the fine grains considered to be sub-grains. However, as the number of passes increases, the area of coarse grains gradually disappeared and the fine grains became more dominant in the microstructures. The result of tensile test for workpieces with each forging pass showed an increase in strength depending on pass number was shown with a slight increase of elongation. The Electron Backscatter Diffraction (EBSD) results exhibited that, the microstructure showed the presence of coarse grains and twins after only 1 pass, while the grains appeared to be significantly refined and uniformly distributed after 3 pass, at which the strength and elongation began to increase, simultaneously.
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Authors and Affiliations

Young-Chul Shin
1
ORCID: ORCID
Seong-Ho Ha
1
ORCID: ORCID
Abdul Wahid Shah
1
ORCID: ORCID

  1. Korea Institute of Industrial Technology (KITECH), Molding & Metal Forming R&D Department, 156 Gaetbeol-ro, Yeonsu-gu, Incheon 21999, Republic of Korea
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Abstract

The as-cast microstructure of ductile cast iron (DI) was investigated using light microscopy (LM) and SEM techniques. Further the influence of hot plastic extrusion at 1000°C with plastic strain in the range of 20-60-80% on the transformation of the as-cast microstructure and on the mechanical properties was studied. Besides this, the microstructure of DI subjected to hot extrusion after the fracture of the corresponding samples induced by compression tests was thoroughly investigated. It was found that compression had a dramatic influence on a shear deformation and hence shear fracture of the compressed samples. It was shown that the shear fracture of the hot deformed ductile iron is accompanied by the occurrence of a narrow zone of severe plastic deformation. The fracture surfaces of the extruded samples subjected to the tensile tests and the compression tests were examined.
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Authors and Affiliations

A.S. Chaus
1
ORCID: ORCID
Ľ. Čaplovič
1
ORCID: ORCID
A.I. Pokrovskii
2
ORCID: ORCID
R. Sobota
1
ORCID: ORCID

  1. Slovak University of Technology, Faculty of Materials Science and Technology, J. Bottu 25, Trnava, 917 24 Slovakia
  2. National Academy of Sciences of Belarus, Physical Technical Institute, 10. Kuprevicha Str., Minsk, 220141 Belarus
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Abstract

This study was undertaken to investigate the effect of severe plastic deformation (SPD) by extrusion combined with reversible torsion (KoBo) method on microstructure and mechanical properties of Al-5Cu and Al-25Cu alloys. The extrusion combined with reversible torsion was carried out using reduction coefficient of λ = 30 and λ = 98. In this work, the microstructure was characterized by light microscopy (LM), scanning electron microscopy (SEM) and scanning transmission electron microscopy (STEM). Compression test and tensile test were performed for deformed alloys. The binary Al-5Cu and Al-25Cu alloys consist of the face cantered cubic (FCC) α phase in the form of dendrites and tetragonal (C16) θ-Al2Cu intermetallic phase observed in interdentritic regions. The increase of Cu content leads to increase of interdentritic regions. The microstructure of the alloys is refined after applying KoB deformation with λ = 30 and λ = 98. Ultimate Tensile Strength (UTS) of Al-5Cu alloy after KoBo deformation with λ = 30 and λ = 98 reached about 200 MPa. UTS for samples of Al-25Cu with λ = 30 and λ = 98 increased compared to Al-5Cu alloy and exceed 320 MPa and 270 MPa respectively. All samples showed increase of plasticity with increase of reduction coefficient. Independently of reduction coefficient, the compressive strain of Al-5Cu alloys is about 60%. The Al-25Cu alloy with λ = 98 showed the value of compressive strain exceed 60%, although for this same alloy but with λ = 30, the compressive strain is only 35%.

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Authors and Affiliations

K. Rodak
A. Brzezińska
J. Sobota
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Abstract

To form the fine micro-structures, the Pr17Fe78B5 magnet powders were produced in the optimized gas atomization conditions and it was investigated that the formation of the textures, microstructures, and the changes in the magnetic properties with increasing the deformation temperatures and rolling directions. Due to the rapid cooling system than the casting process, the homogenous microstructures were composed of the Pr-rich and Pr2Fe14B without any oxides and α-Fe and enables grain refinement. The pore ratios were 2.87, 1.42, and 0.22% at the deformation temperatures of 600, 700, 800°C, respectively in the rolled samples to align the c-axis which is the magnetic easy axis. Because Pr-rich phase cannot flow into the pore with a liquid state at low temperature, the improvement of pore densification was gradually observed with increasing deformation temperature. To confirm the magnetic decoupling effects of Pr2Fe14B phases by Pr-rich phases, the magnetic properties were investigated in rolled samples produced at the deformation temperature of 800°C. Although the remanent field is slightly decreased by 30%, the coercivity fields increased by about 2 times than that previous casted ingot. It is suggested that the gas atomization method can be suitable for fabricating grain refined and pure PrFeB magnets, and the plastic deformation conditions and rolling directions are a critical role to manipulate microstructure and magnetic properties.
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Bibliography

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Authors and Affiliations

Ju-Young Cho
1 2
ORCID: ORCID
Myung-Suk Song
1
ORCID: ORCID
Yong-Ho Choa
2
ORCID: ORCID
Taek-Soo Kim
1 3
ORCID: ORCID

  1. Research Institute of Advanced Manufacturing Technology, Korea Institute of Industrial Technology, 156 Gaetbeol-ro (Songdo-dong), Yeonsu-Gu, Incheon 21999, Korea
  2. Hanyang University, Department of Material Science and Chemical Engineering, Ansan 15588, Korea
  3. University of Science and Technology, Critical Materials and Semi-Conductor Packaging Engineering, Daejeon 3413, Republic of Korea
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Abstract

The research presented in this paper concerns the influence of the rate of plastic deformation generated directly in the processes of severe plastic deformations on the microstructure and properties of three metals: copper, iron and zinc. The equal channel angular pressing (ECAP) method was used, and it was performed at a low plastic deformation rate of ∼ 0.04 s−1. The high plastic strain rate was obtained using the hydrostatic extrusion (HE) method with the deformation rate at the level of ∼ 170 s−1. For all three tested materials different characteristic effects were demonstrated at the applied deformation rates. The smallest differences in the mechanical properties were observed in copper, despite the dynamic recrystallization processes that occurred in the HE process. In Armco iron samples, dynamic recovery processes in the range of high plastic deformation rates resulted in lower mechanical properties. The most significant effects were obtained for pure zinc, where, regardless of the method used, the microstructure was clearly transformed into bimodal after the ECAP process, and homogenized and refined after the HE process. After the HE process, the material was transformed from a brittle state to a plastic state and the highest mechanical properties were obtained.
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Authors and Affiliations

Mariusz Kulczyk
1
ORCID: ORCID
Monika Skorupska
1
Jacek Skiba
1
Sylwia Przybysz
1
Julita Smalc-Koziorowska
1

  1. Institute of High Pressure Physics of the Polish Academy of Sciences UNIPRESS, Sokołowska 29/37, 01-142 Warsaw, Poland
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Abstract

In this scientific publication, research results of two newly developed hot-rolled Fe-Mn-Al-C (X105) and Fe-Mn-Al-Nb-Ti-C (X98) types of steel were compared. These types of steel are characterized by an average density of 6.68 g/cm³, a value 15% lower compared to conventional structural steel. Hot rolling was carried out on a semi-industrial line to evaluate the effect of hot plastic deformation conditions with different cooling variants on the structure. The detailed analysis of phase composition as well as microstructure allows us to state that the investigated steel is characterized by an austenitic-ferritic structure with carbides precipitates. The results of the transmission electron microscopy (TEM) tests of both types of steel after hot rolling showed the occurrence of various deformation effects such as shear bands, micro bands, and lens twins in the microstructure. Based on the research undertaken with the use of transmission electron microscopy, it was found that the hardening mechanism of the X98 and X105 steel is deformation-induced plasticity by the formation of shear bands (SIP) and micro shear bands (MBIP).
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Bibliography

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Authors and Affiliations

Liwia Sozańska-Jędrasik
1
Wojciech Borek
2
ORCID: ORCID
Janusz Mazurkiewicz
2

  1. Łukasiewicz Research Network–Institute for Ferrous Metallurgy, Department of Investigations of Properties and Structure of Materials, ul. K. Miarki 12-14, Gliwice 44-100, Poland
  2. Silesian University of Technology, Department of Engineering Materials and Biomaterials, ul. Konarskiego 18a, Gliwice 44-100, Poland
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Abstract

Microstructure and texture of the CuCr0.6 alloy processed by rolling with cyclic movement of rolls (RCMR) at room temperature were investigated. The RCMR processing was applied for the samples in different initial conditions in the solid solution followed by quenching into iced water at 1000oC for 3 h and in aging treatment conditions performed at 500oC for 2 h and at 700oC for 24 h. Application of the solution and aging processes prior to RCMR deformation results in the partial dissolution of Cr particles into the Cu matrix and precipitation of the second phase particles. RCMR processing with value of the total effective strain (εft) of 5 was introduced to the material. It was found that the RCMR method is effective in texture weakening. The obtained results revealed that there is a large similarity in texture orientations after RCMR processing independently of heat treatment conditions. Cyclic character of deformation leads to an incomplete transition of LAB to HAB.

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Authors and Affiliations

A. Urbańczyk-Gucwa
A. Brzezińska
B. Adamczyk-Cieślak
ORCID: ORCID
K. Rodak
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Abstract

Two strength-age hardening aluminum-lithium alloys: Al-2.3wt%Li and Al-2.2wt%Li-0.1wt%Zr in two different heat treatment conditions: solution state (S) and additionally in aging state (A) were severely plastically deformed by rolling with cyclic movement of rolls (RCMR) method to produce ultrafine – grained structure. Two thermo-mechanical treatments were used: (S+A+RCMR) and (S+RCMR+A+RCMR). To investigate the combined effect of plastic deformation and heat treatment, tensile tests were performed. Microstructural observations were undertaken using scanning transmission electron microscopy (STEM), and scanning transmission electron microscopy (SEM) equipped with electron backscattering diffraction detector (EBSD). Based on the obtained results, it can be deduced that maximum mechanical properties as: yield strength (YS) and ultimate tensile strength (UTS) could be achieved when the microstructure of alloys is in (S+A+RCMR) state. For samples in (S+RCMR+A+RCMR) state, ductility is higher than for (S+A+RCMR) state. The microstructural results shows that the favourable conditions for decreasing grain size of alloys is (S+A+RCMR) state. Additionally, in this state is much greater dislocation density than for (S+RCMR+A+RCMR) state. The microstructure of alloys in (S+RCMR+A+RCMR) state is characterized by grains/subgrains with higher average diameter and with higher misorientation angles compared with (S+A+RCMR) state.

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Authors and Affiliations

A. Brzezińska
A. Urbańczyk-Gucwa
R. Molak
K. Rodak
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Abstract

The paper has presented the results of theoretical studies and experimental tests of the plastic deformation of multi-layered Ti/Al/Mg specimens. Theoretical studies were carried out using the Forge2011® computer program. Physical modeling, on the other hand, was performed using the Gleeble3800 simulator. Cuboidal specimens were cut off from the plates obtained in the explosive welding method. Based on the obtained investigation results it has been found non uniform deformation of the particular layer as a result their different value of flow stress.

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Authors and Affiliations

S. Mróz
A. Stefanik
P. Szota
M. Kwapisz
M. Wachowski
ORCID: ORCID
L. Śnieżek
ORCID: ORCID
A. Gałka
Z. Szulc
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Abstract

NdFeB anisotropic sintered permanent magnets are typically fabricated by strip casting or melt spinning. In this study, the plastic deformability of an NdFeB alloy was investigated to study the possibility of fabricating anisotropic sintered magnets using gas atomized powders. The results show that the stoichiometric composition Nd12Fe82B6 softens at high temperatures. The aspect ratio and orientation factor of Nd12Fe82B6 billets after plastic deformation were found to increase with increasing plastic deformation temperature, particularly above 800℃. This confirms that softening at high temperatures can lead to plastic deformation of Nd2Fe14B hard magnetic phases.

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Authors and Affiliations

Ju-Young Cho
ORCID: ORCID
Yong-Ho Choa
ORCID: ORCID
Sun-Woo Nam
ORCID: ORCID
Rasheed Mohammad Zarar
Taek-Soo Kim
ORCID: ORCID
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Abstract

Oxide-dispersion-strengthened high-entropy alloys were produced by hot-pressing a ball-milled mixture of Y2O3 and atomized CoCrFeMnNi powder. The effect of milling duration on grain size reduction, oxide formation behavior, and the resulting mechanical properties of the alloys was studied. Both the alloy powder size and Y2O3 particle size decreased with milling time. Moreover, the alloy powder experienced severe plastic deformation, dramatically generating crystalline defects. As a result, the grain size was reduced to ~16.746 nm and in-situ second phases (e.g., MnO2 and σ phase) were formed at the defects. This increased the hardness of the alloys up to a certain level, although excessive amounts of in-situ second phases had the reverse effect.
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Authors and Affiliations

Yongwook Song
1
ORCID: ORCID
Daeyoung Kim
1
ORCID: ORCID
Seungjin Nam
1
ORCID: ORCID
Kee-Ahn Lee
2
ORCID: ORCID
Hyunjoo Choi
1
ORCID: ORCID

  1. Kookmin University, School of Materials Science and Engineering, Seoul, Republic of Korea
  2. Inha University, Department of Materials Science and Engineering, Incheon 22212, Republic of Korea

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