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Number of results: 89
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Abstract

Celem pracy była wstępna charakterystyka (mineralogiczna, chemiczna, teksturalna) odpadów poflotacyjnych, stanowiących surowiec uboczny (odpadowy) przy uzyskiwaniu koncentratów cynkowo-ołowiowych, pod kątem dalszych analiz nad możliwością ich perspektywicznego (eksperymentalnego) wykorzystania jako sorbentów gazów kwaśnych (SO2 i CO2). Składowisko tych odpadów jest własnością ZGH 'Bolesław' w Bukownie. Materiał badawczy stanowiła próbka odpadów poflotacyjnych pobrana ze stawu osadowego nr 1, leżącego w południowej części Stawu Zachodniego. Charakterystyka wytypowanych do badań materiałów obejmowała podstawowe badania mineralogiczne (XRD, SEM-EDS), analizy chemiczne (oznaczenie zawartości wilgoci analitycznej, zawartości strat prażenia, podstawowego składu chemicznego, jak też pierwiastków śladowych) oraz wyznaczenie podstawowych parametrów teksturalnych (powierzchnia właściwa BET, rozkład i wielkość porów). Badania mineralogiczne wykazały, że materiał odpadowy stanowią głównie minerały węglanowe (w przewadze kalcyt, dolomit, ankeryt) oraz minerały stanowiące pozostałość po niewyflotowanych kruszcach (w przewadze galena, sfaleryt). Analiza chemiczna pozwoliła stwierdzić, iż w analizowanej próbce dominują związki wapnia, magnezu i żelaza uwarunkowane przewagą minerałów węglanowych w badanych odpadach. Wśród pierwiastków śladowych przeważa arsen, następnie mangan i bar, występujące jednak w ilości nie przekraczającej 1%. Analiza teksturalna wykazała, że materiał badawczy charakteryzuje się niską powierzchnią właściwą i dużymi rozmiarami cząstek. Przeprowadzone badania sugerują, że analizowany materiał charakteryzuje się ubogimi właściwościami adsorpcyjnymi, aczkolwiek mógłby on znaleźć zastosowanie w metodach odsiarczania, jak też neutralizacji dwutlenku węgla (karbonizacja). Należałoby jednak w tym celu przeprowadzić dodatkowe badania wymywalności metali ciężkich w środowisku kwasowym, jak też zastosować domieszki innych składników, takich jak cement czy zeolity, w celu immobilizacji niebezpiecznych składników odpadów.

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Authors and Affiliations

Magdalena Wdowin
Agnieszka Gruszecka
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Abstract

Zinc oxide is considered an outstanding photocatalyst candidate, but its low photo-corrosion resistance is a problem to be solved. In the ZnO-ZnS core-shell structure, ZnS acts as a protective layer for the ZnO core, and thus, it can enhance stability and long-term performance. The ZnO-ZnS core-shell structure is synthesized into various nanoscale morphologies with high specific surface areas to improve photocatalytic efficiency. However, they are easily agglomerated and are hard to separate from reaction media. In this study, micro-sized bumpy spheres of ZnO-ZnS core-shell structure were prepared via facile chemical transformation of as-prepared ZnO. After sulfurization of the ZnO template, it was confirmed through SEM, TEM, EDS, and XPS analysis that a uniform ZnS shell layer was formed without significant change in the initial ZnO morphology. The ZnO-ZnS core-shell microsphere has shown superior efficiency and stability in the photocatalytic degradation of Rhodamine B compared with pristine ZnO microspheres
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Authors and Affiliations

Hee Yeon Jeon
1
ORCID: ORCID
Mijeong Park
1
ORCID: ORCID
Seungheon Han
1
ORCID: ORCID
Dong Hoon Lee
1
ORCID: ORCID
Young-In Lee
2
ORCID: ORCID

  1. Seoul National University Of Science and Technology, Department Of Materials Science and Engineering, Seoul 01811, Republic Of Korea
  2. Seoul National University of Science and Technology, Department of Materials Science and Engineering, Seoul 01811, Republic of Korea
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Abstract

The Bulletin of the Polish Academy of Sciences: Technical Sciences (Bull.Pol. Ac.: Tech.) is published bimonthly by the Division IV Engineering Sciences of the Polish Academy of Sciences, since the beginning of the existence of the PAS in 1952. The journal is peer‐reviewed and is published both in printed and electronic form. It is established for the publication of original high quality papers from multidisciplinary Engineering sciences with the following topics preferred: Artificial and Computational Intelligence, Biomedical Engineering and Biotechnology, Civil Engineering, Control, Informatics and Robotics, Electronics, Telecommunication and Optoelectronics, Mechanical and Aeronautical Engineering, Thermodynamics, Material Science and Nanotechnology, Power Systems and Power Electronics.

Journal Metrics: JCR Impact Factor 2018: 1.361, 5 Year Impact Factor: 1.323, SCImago Journal Rank (SJR) 2017: 0.319, Source Normalized Impact per Paper (SNIP) 2017: 1.005, CiteScore 2017: 1.27, The Polish Ministry of Science and Higher Education 2017: 25 points.

Abbreviations/Acronym: Journal citation: Bull. Pol. Ac.: Tech., ISO: Bull. Pol. Acad. Sci.-Tech. Sci., JCR Abbrev: B POL ACAD SCI-TECH Acronym in the Editorial System: BPASTS.

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Authors and Affiliations

Agata Jarzynka
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Abstract

Autor definiuje pojęcie kultury przez odniesienie do szczególnej kategorii znaczeń normatywnych, czyli wartości. System wartości zorganizowany jest wokół trzech wartości najbardziej ogólnych i fundamentalnych: prawdy, dobra i piękna. Odpowiednio mówić można o trzech domenach kultury: kulturze poznawczej, kulturze moralnej i kulturze estetycznej. Desygnatami kultury poznawczej są przekonania, poglądy, opinie podzielane przez członków społeczeństwa. Desygnatami kultury moralnej są relacje łączące jednostki w przestrzeni międzyludzkiej. Desygnatami kultury estetycznej są szczególnego typu wytwory należące do sztuki artystycznej lub użytkowej. Podobieństwo wartości w każdym z tych trzech obszarów stanowi silny czynnik wytwarzający więzi społeczne i wspólnoty, a także tożsamości społeczne. Kultura jest fundamentem żywej i bogatej tkanki społecznej, społeczeństwa obywatelskiego.

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Authors and Affiliations

Piotr Sztompka
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Abstract

Nanostructured systems based on ZnO nanoparticles composite systems/polymer fibers have attracted a lot of attention in the last years because of their applications in multiple areas. Nanofibres based on polymers are used in many domains such as nanocatalysis, controlled release of medicines, environmental protection and so on. This work show the synthesis of cellulose acetate butyrate (CAB) nanofiber useful as substrates for growing ZnO nanocrystals and that ZnO is an unorganic metal oxide nanoparticle used to improve the piezoelectric properties of the polymer. The piezoelectric propertiesof ZnO-doped polymeric was investigated with atomic force microscopy and measurements were performed, in contact technique, in piezoelectric response mode (PFM).In order to analyze the structural and textural features, the obtained materials were characterized using advanced physical-chemical techniques such as X-ray diffraction (XRD), Atomic Force Microscopy (AFM), Scanning Electron Microscopy (SEM). The XRD patterns show the characteristic reflections of ZnO with a hexagonal type wurtzit structure and the broad peaks of the polymer. The SEM images reveal the presence of ZnO nanoparticles on top of the polymer nanofibres.In most ZnO-based nanocomposites their morphology is uncontrolled (agglomerated granules), but in ase of using cellulose acetobutyrate this becomes controlled by observing through flower-like structures SEM and AFM) The study of the functional properties of ZnO/polymer fiber composite systems showed that they have piezoelectric properties which give them the characteristics of smart material with possible sensor and actuator applications.Recent literature reports that the synthesis and characterization of ZnO-polymer nanocomposites are more flexible materials for various applications.
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Authors and Affiliations

G. Calin
1
ORCID: ORCID
L. Sachelarie
1
ORCID: ORCID
N. Olaru
2
ORCID: ORCID

  1. Apollonia University of Iasi, Faculty of Dental Medicine, 11 Pacurari Str., 700511, Iasi, Romania
  2. Institute of Macromolecular Chemistry “Petru Poni” Iasi, Aleea Grigore Ghica Voda,41A, 700487, Iasi, Romania
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Abstract

The paper presents research of metallic glass based on a Mg72Zn24Ca4 alloy. Metallic glass was prepared using induction melting and further injection on a spinning copper wheel. The X-ray diffractometer and differential scanning calorimeter (DSC) were used to investigate the phase transformation of the amorphous ribbon. The heat released in the crystallization process, during isothermal annealing, based on the differential scanning calorimeter investigation, was determined to be 166.18 Jg-1. The effect of isothermal annealing temperature on the kinetics of the amorphous alloy crystallization process using differential scanning calorimeter was investigated. For this purpose, two isothermal annealing temperatures were selected. The incubation time decreases as the temperature of the isothermal annealing increases from 300 to 252 seconds. The same relationship is visible in the case of duration of the phase transformation, which also decreases as the temperature of the isothermal annealing increases from 360 to 228 seconds. The obtained results show a significant influence of isothermal annealing temperature on the degree of phase transformation.

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Authors and Affiliations

J. Lelito
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Abstract

For many years, learning the competences to teach mathematics in early education at university has been associated with the ability to reproductively apply methodological guidelines. Currently, however, the need to not only understand the mathematical meanings given by teachers, but also students of the specialty, are seen to be important. This article attempts to engage in an interpretive line of thinking with regard to mathematics education, coming from the perspective of students learning to be early education teachers. Their understanding of the contexts for learning mathematical concepts, as well as their sensitivity to the processes of constructing mathematical knowledge by very young pupils, being a way of predicting what educational activities will be undertaken in the classroom in the future. This text is the result of qualitative analyses of written essays of early education students, where respondents had to make conceptualizations of their beliefs by justifying the selection of particular declarative statements. Students’ mathematical meanings were also uncovered in their strategies for solving mathematical problems for very young pupils. Moreover, the results of this analyses provides a context for reading the students’ understanding of mathematics learning processes.

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Authors and Affiliations

Alina Kalinowska
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Abstract

Rozmowa z Kazimierą Szczuką o prof. Marii Janion – wizjonerce humanistyki, rewolucjonistce romantyzmu, skromnej mistrzyni swoich uczniów.
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Authors and Affiliations

Kazimiera Szczuka
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Abstract

Hybrid filter material was obtained via modification of polypropylene (PP) nonwoven with nanosize zinc oxide particles of a high aspect ratio. Modification was conducted as a three-step process, a variant of hydrothermal method used for synthesis of nano-ZnO, adopted for coating three dimensional polymeric nonwoven filters. The process consisted of plasma treatment of nonwoven to increase its wettability, deposition of ZnO nanoparticles and low temperature hydrothermal growth of ZnO rods. The modified nonwovens were investigated by a high resolution scanning electron microscopy (HR-SEM). It has been found that the obtained hybrid filters offer a higher filtration efficiency, in particular for so called most penetrating particle sizes.

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Authors and Affiliations

Szymon Jakubiak
Justyna Tomaszewska
Anna Jackiewicz
Jakub Michalski
Krzysztof J. Kurzydłowski
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Abstract

The aim of this paper was to determine the effect of heat treatment for the corrosion resistance of the ZnAl40Ti2Cu alloy under “acid rain” conditions. ZnAl40TiCu alloy after supersaturation and after supersaturation and aging was studied. Potentiodynamic studies, potentiostatic studies and studies on structure of the alloy top layer of samples after corrosion tests were carried out. These investigations indicated a significant influence of heat treatment on corrosion resistance of the ZnAl40Ti2Cu alloy. The highest increase in corrosion resistance comparing to the alloy in the as-cast condition may be obtained by supersaturation. A significant influence of the aging temperature and time on corrosion resistance was proved.
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Authors and Affiliations

R. Michalik
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Abstract

Tytułowe kategorie znaczenia, rozumowania i normatywności wyznaczają temat i cel artykułu. Jego celem jest odpowiedź na główne pytanie: czy między znaczeniem i rozumowaniem istnieje jakiś związek? A jeżeli tak, to jeden, czy wiele? Jaki? Jakie? Udzielając pozytywnej odpowiedzi, w punkcie (1) prezentuję definicję rozumowania (wnioskowania), a w punkcie (2) rozróżniam i przedstawiam związki formalne oraz pozaformalne. Związki formalne są opracowywane przez logikę. Nazwy – z określonymi znaczeniami, czyli pojęciami – tworzą zdania (związki wewnątrzzdaniowe). Ich znaczenia to sądy. Zdania pełnią funkcje przesłanek i wniosku w rozumowaniu (związki międzyzdaniowe). Do związków pozaformalnych można zaliczyć: związek między zdaniem a stanem rzeczy, do którego zdanie się odnosi (referencja i łącząca się z nią własność prawdziwości zdania). Inne związki pozaformalne to: związek przyczynowo-skutkowy, związek następstwa czasowego, związek przestrzenny i związki normatywne.

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Authors and Affiliations

Robert Kublikowski
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Abstract

W artykule zestawione zostają dwie koncepcje okazjonalności. Pierwsza, standardowa i wąska, okazjonalność wyrażenia wiąże ściśle z jego znaczeniem i regulowanym przez nie związkiem kontekstu z określoną rolą wyrażenia. Druga, szersza i wywodząca się z prac Jerzego Pelca, określa okazjonalność w kategoriach potencjalnej zmienności ogólnej charakterystyki semiotycznej wyrażenia przy zachowaniu jego znaczenia. W tekście wprowadzone zostaje pojęcie matrycy pragmatycznej, które służy do schematycznego przedstawiania zmienności kontekstowej. Rekapituluję także krótko poglądy Jerzego Pelca na znaczenie (sposób użycia) i użycie oraz wskazuję krótko na związki jego podejścia ze współczesnymi debatami wokół kontekstualizmu oraz statusu wypowiedzi niezdaniowych.
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Authors and Affiliations

Tadeusz Ciecierski
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Abstract

The main reason of a cavitational destruction is the mechanical action of cavitation pulses onto the material’s surface. The course

of cavitation destruction process is very complex and depends on the physicochemical and structural features of a material. A resistance

to cavitation destruction of the material increases with the increase of its mechanical strength, fatigue resistance as well as hardness.

Nevertheless, the effect of structural features on the material’s cavitational resistance has been not fully clarified. In the present paper,

the cavitation destruction of ZnAl4 as cast alloy was investigated on three laboratory stands: vibration, jet-impact and flow stands.

The destruction mechanism of ZnAl4 as cast alloy subjected to cavitational erosion using various laboratory stands is shown in the present

paper.

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Authors and Affiliations

R. Jasionowski
D. Zasada
W. Polkowski
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Abstract

We present Al2O3-ZnAl2O4-ZnO nanostructure, which could be a prominent candidate for optoelectronics, mechanical and sensing applications. While ZnO and ZnAl2O4 composites are mostly synthesized by sol-gel technique, we propose a solid-vapor growth mechanism. To produce Al2O3-ZnAl2O4-ZnO nanostructure, we conduct ZnO:C powder heating resulting in ZnO nanowires (NWs) growth on sapphire substrate and ZnAl2O4 spinel layer at the interface. The nanostructure was examined with Scanning Electron Microscopy (SEM) method. Focused Ion Beam (FIB) technique enabled us to prepare a lamella for Transmission Electron Microscopy (TEM) imaging. TEM examination revealed high crystallographic quality of both spinel and NW structure. Epitaxial relationships of Al2O3-ZnAl2O4 and ZnAl2O4-ZnO are given.
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Authors and Affiliations

W. Zajkowska-Pietrzak
1
ORCID: ORCID
J. Turczyński
1
ORCID: ORCID
B. Kurowska
1
ORCID: ORCID
H. Teisseyre
1
ORCID: ORCID
K. Fronc
1
ORCID: ORCID
J. Dąbrowski
1
ORCID: ORCID
S. Kret
1
ORCID: ORCID

  1. Institute of Physics Polish Academy of Sciences, 32/46 Lotników Av., 02-668 Warszawa, Poland
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Abstract

High-power terahertz sources operating at room-temperature are promising for many applications such as explosive materials detection, non-invasive medical imaging, and high speed telecommunication. Here we report the results of a simulation study, which shows the significantly improved performance of room-temperature terahertz quantum cascade lasers (THz QCLs) based on a ZnMgO/ZnO material system employing a 2-well design scheme with variable barrier heights and a delta-doped injector well. We found that by varying and optimizing constituent layer widths and doping level of the injector well, high power performance of THz QCLs can be achieved at room temperature: optical gain and radiation frequency is varied from 108 cm−1 @ 2.18 THz to 300 cm−1 @ 4.96 THz. These results show that among II–VI compounds the ZnMgO/ZnO material system is optimally suited for high-performance room-temperature THz QCLs.

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Authors and Affiliations

V.P. Sirkeli
H.L. Hartnagel
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Abstract

The aim of the investigation was to determine the impact of the presence of Zn in concentrations of sludges applied in agriculture (exceeding concentrations determined in sludges drained from the treatment plant) 011 the disappearance of PAHs in sewage sludge stored under aerobic conditions. The studies were carried out using dewatered and biochemically stabilized sludges. The changes in the concentration of PAHs were studied in four series: in sludge samples taken after filter press, in sludge with the addition of a standard PAH mixture. in sludge with Zn added, in sludge with the addition of both the standard PAH mixture and Zn. The standard PAH mixture used in the studies contained 16 compounds in benzene - dichloromethane (I: ł) solution with a concentration of 32000 ug/cm' of 16 PAHs. Zn was added to the sludge samples as a solution of chloride zrnc. the final amount was below 2500 mg Zn/kg d.m. (taking into consideration the initial concentrations) The sludge samples were incubated for 90 days at 20°C with limitless access of oxygen. The determination of PAHs in sludge samples was done in duplicates at the beginning of the experiment (the initial concentration) and then six times at I 5-day intervals (after 15. 30. 45. 60. 75 and 90 days). A gas chromatography-mass spectrometry (GC-MS) was used to qualify and quantify the PAHs. I 6 PAI-ls listed by EPA were identified
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Authors and Affiliations

Maria Włodarczyk-Makuła
Marta Janosz-Rajczyk
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Abstract

During the rutting season, stag semen is accompanied by a sticky, dense secretion called yellow fraction (YF). There is little information about the role, biology, physiology, and most importantly, the composition of this fluid. The aim of this study was to isolate and identify zinc ions (ZnBPs) and heparin binding proteins (HBPs) from YF of the red deer ( Cervus elaphus L.). Using liquid chromatography, the presence of 6 fractions of ZnBPs (71, 65, 55, 16, 14 and 12 kDa) and 22 fractions of HBPs (163, 140, 96, 78, 71, 65, 55, 49, 33, 31, 26, 25, 24, 22, 18, 16, 13, 12, 11, 10, 9 and 8 kDa) in YF proteome was demonstrated. By means of two-dimensional electrophoreses and MALDI-TOF/TOF mass spectrometry some of them were then identified. Amongst ZnBPs the following were identified: glutaminyl-peptide cyclotransferase, inhibitor of carbonic anhydrase-like, potassium voltage-gated channel subfamily E member 2, WD repeat-containing protein 38 isoform X4. Amongst the HBPs metalloproteinase inhibitor 2 (TIMP2), seminal plasma glycoprotein PSP-I and adseverin (scinderin) were identified. Identifying all ZnBPs and HBPs present in YF may broaden up-to-date knowledge concerning the biology, physiology and preservation of red deer semen.
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Authors and Affiliations

A. Orzołek
1
K. Dyrda
1
K. Rafalska
1
P. Wysocki
1
W. Kordan
1
W. Giżejewski
2

  1. Department of Animal Biochemistry and Biotechnology, University of Warmia and Mazury, Oczapowskiego 5, 10-719 Olsztyn, Poland
  2. Institute of Animal Reproduction and Food Research, Polish Academy of Sciences, Tuwima 10, 10-748 Olsztyn, Poland
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Abstract

This paper presents the effect of the addition of Ti to the zinc bath. Hot-Dip Galvanizing was carried out on a machined ductile cast iron substrate. The process was carried out at 550°C. Experimental baths A, B and C contained 0.01%, 0.05% and 0.1%Ti, respectively. Metallographic samples were prepared to reveal the microstructure of the coatings. Thickness measurements of the obtained coatings were carried out, and graphs of the approximate crystallization kinetics of the zinc coating were prepared. High-temperature galvanization carried out on the treated surface led to the release of graphite beads from the metal matrix and their diffusion into the coating. This phenomenon can have an adverse effect on the continuity of the coating and its adhesion to the substrate. Crystallization of the δ phase was observed in the coating, and at longer immersion times – a mixture of two-phase δ1 and η phases. With increasing Ti content in the bath, a deterioration in the casting properties of the bath was observed.
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Bibliography

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Authors and Affiliations

Karolina Bracka-Kęsek
1
ORCID: ORCID
Andrzej Szczęsny
1
ORCID: ORCID
Dariusz Kopyciński
1
ORCID: ORCID
Edward Guzik
1
ORCID: ORCID

  1. AGH University of Science and Technology, Department of Foundry Engineering, Al. Mickiewicza 30, 30-059 Kraków, Poland
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Abstract

A n-type semiconductor ZnO has high transmittance features, excellent chemical stability and electrical properties. It is also commonly used in a range of fields, such as gas sensors, photocatalysts, optoelectronics, and solar photocell. Magnesium-doped zinc oxide (Mg-ZnO) nano powders were effectively produced using a basic chemical precipitation process at 45°C. Calcined Mg-ZnO nano powders have been characterized by FTIR, XRD, SEM-EDX and PL studies. XRD measurements from Mg-ZnO revealed development of a crystalline structure with an average particle size of 85 nm and SEM analysis confirmed the spherical morphology. Electrochemical property of produced Mg-ZnO nanoparticles was analyzed and the specific capacitance value of 729 F g–1 at 0.5 A g–1 current density was recorded and retained a specific capacitance ~100 percent at 2 A g–1 current density.
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Authors and Affiliations

S. Arul
1
ORCID: ORCID
T. Senthilnathan
2
ORCID: ORCID
V. Jeevanantham
3
ORCID: ORCID
K.V. Satheesh Kumar
4
ORCID: ORCID

  1. Jai Shriram Engineering College, Department of Physics, Tirupur-638660, Tamilnadu, India
  2. Sri Venkateshwara College of Engineering, Department of Applied Physics, Sriperumbudur-602117, Tamilnadu, India
  3. Vivekanandha College of Arts & Sciences for Women, Department of Chemistry, Tiruchengode 637205, Tamilnadu, India
  4. Kongu Engineering College, Department of Mechanical Engineering, Erode-638060, Tamilnadu, India
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Abstract

This study suggests a new way to modify the size and morphology of Al-Fe phases in modified AA 7075 by using an Fe-Mn solid solution powder as the precursor. When Fe and Mn are added in the form of a solid solution, the diffusion of Fe and Mn toward the Al is delayed, thus altering the chemical composition and morphology of the precipitates. The fine, spherical precipitates are found to provide a good balance between strength and ductility compared to the case where Fe and Mn are separately added.
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Authors and Affiliations

Min Sang Kim
1 2
ORCID: ORCID
Dae Young Kim
3
ORCID: ORCID
Young Do Kim
1
ORCID: ORCID
Hyun Joo Choi
3
ORCID: ORCID
Se Hoon Kim
2
ORCID: ORCID

  1. Hanyang University, Department of Materials Science & Engineering, Seoul, Republic of Korea
  2. Metallic Material R&D Center, Korea Automotive Technology Institute, Cheonan-si, Republic of Korea
  3. Kookmin University, School of Materials Science and Engineering, Seoul, Republic of Korea
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Abstract

Through the powder metallurgy technique, alloys of the eutectic composition of the Zn-Al system were manufactured (22.3 wt.%Al), reinforced with Ag additions (0.5, 1, 2.5, 5 wt.%), with subsequent annealing heat treatment at three different temperatures; 100, 150 and 200°C for 1 hr. X-ray diffraction, optical microscopy and mechanical tests were performed on the resulting samples. The addition of Ag favors the formation of alpha and beta compounds with Al and Zn respectively, which improves the compressive strength of the alloy. However, with the presence of Ag the hardness is decreased. On the other hand, the application of an annealing heat treatment, shows no significant effect on the evaluated properties of the alloy. The microstructure of the alloys resulted in the presence of very small grains smaller than 1 mm and with rounded morphology.
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Authors and Affiliations

Miguel Angel Rubio-Padrón
1
ORCID: ORCID
Olga Alondra Echartea-Reyes
1
Carlos A. Calles-Arriaga
1
ORCID: ORCID
Enrique Rocha-Rangel
1
ORCID: ORCID

  1. Universidad Politécnica de Victoria, Ciudad Victoria, México
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Abstract

The report presents research efforts on the synthesis of Zn/MoS2 composite coatings by electrochemical reduction from a sulphate-borate bath containing MoS2 powder as a dispersion phase at various concentrations. The structure of the Zn/MoS2 composite coatings was characterised and the effect of MoS2 particles embedded on their microhardness was evaluated. The coatings produced are characterized by a compact, homogeneous structure and a good connection to a steel substrate. The incorporation of MoS2 particles into the zinc matrix has an influence on the structure and morphology of the Zn/MoS2 composite coatings. It was found that the presence of MoS2 particles increases surface roughness along with coating hardness. The incorporation of the MoS2 particles into the zinc matrix slightly improves the corrosion resistance compared to Zn coatings, making the corrosion potential shift towards more electropositive values.

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Authors and Affiliations

K. Szmigielska
M. Trzaska

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