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Abstract

Microwave sintering process was employed to agglomerate ferromanganese alloy powders. The effects of sintering temperature, holding time and particle size composition on the properties and microstructure of sintering products were investigated. The results was shown that increasing sintering temperature or holding time appropriately is beneficial to increase the compressive strength and volume density. SEM and EDAX analysis shows that the liquid phase formed below the melting point in the sintering process, which leads to densification. XRD patterns indicate that the main reaction during microwave sintering is the decarbonization and carburization of iron carbide phase. The experiment demonstrate that the optimum microwave sintering process condition is 1150°C, 10 min and 50% content of the powders with the size of –75 μm
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Authors and Affiliations

Lei Li
Libo Zhang
Linqing Dai
Hongbo Zhu
Guo Chen
Jinhui Peng
Qin Guo
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Abstract

In this study, Hydroxyapatite (HAp) is extracted from the Rihu fish scales which are generally dumped as garbage. The aluminium composite was fabricated through the powder metallurgy technique by reinforcing HAp (0, 5, 10 and 15 wt%) as a reinforcement. The fabricated samples were sintered through microwave sintering at 530℃ for 15 min under an argon gas environment. The fabricated composites were subjected to X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM) and Energy Dispersive Spectroscopy (EDS) analysis to confirm the constituting elements and to describe the reinforcement dispersion in the matrix. Uniform reinforcement dispersion was observed for the composite reinforces with 5%HAp, 10%HAp particles. The mechanical characterization results reveal that the Al-10% HAp composite exhibits a microhardness value of 123 ± 3 Hv and maximum ultimate tensile strength of 263 ± 10 MPa and 299 ± 9 MPa compression strength was obtained due to the presence of a strong bond among the aluminium and HAp particles.
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Authors and Affiliations

V.S.S. Venkatesh
1
ORCID: ORCID
Kalapala Prasad
2
ORCID: ORCID
Ashish B. Deoghare
3
ORCID: ORCID

  1. GMR Institute of Technology, Rajam, India
  2. University College of Engineering, JNTU Kakinada, India
  3. National Institute of Technology Silchar, Assam, India
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Abstract

The present research addresses the low-temperature sintering of 4% kaolin clay reinforced aluminium composite using susceptor-aided microwave sintering at 2.45 GHz frequency. Kaoline clay the naturally available mineral in the north-eastern regions of india. The study aims to convert this kaoline clay into the value added product with enhanced mechanical properties. The Al-x% Kaolin (x = 2, 4, 6, 8, 10) composite was fabricated through the powder metallurgy process by the application of 600 MPa compaction pressure. The composite corresponding to optimum ultimate tensile strength (U.T.S) was subjected to single-mode cavity microwave-assisted sintering by varying the sintering temperatures as 500°C, 550°C and 600°C. The effect of incorporating kaolin clay on the dielectric characteristics of composite powders, as well as the effect of sintering temperature on the microstructural changes and mechanical characteristics of Al-4%Kaolin composites were also examined. Results concluded that the addition of 4 wt% kaolin powder improves the dielectric characteristics of the composite powder. The maximum Hardness. Compression strength and U.T.S of 97 Hv, 202 MPa and 152 MPa respectively achieved for the Al-4% Kaolin composite sintered at 550°C. The higher fracture toughness of 9.56 Ma. m1/2 reveals the ductile fracture for the composite sintered at 550°C.
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Authors and Affiliations

V.S.S. Venkatesh
1
ORCID: ORCID
Sunil Kumar
2
ORCID: ORCID
Lokeswar Patnaik
3
ORCID: ORCID

  1. G.M.R Institute of Technology, Rajam, Andhra Pradesh, India
  2. Department of Mechanical Engineering, Amrita School of Engineering, Amrita Vishwa Vidyapeetham, Chennai, India
  3. School of Mechanical Engineering, Sathyabama Institute of Science and Technology (Deemed to Be University), Chennai, Tamil Nadu, 600 119, India

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