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Number of results: 21
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Abstract

The orientations of recrystallization nuclei and their adjacent as-deformed regions have been characterised in deformed single crystals of different metals (Ag, Cu, Cu-2%wt.Al and Cu-8%wt.Al) in which twinning and/or shear banding occur. {112}<111> oriented crystals of these metals have been compressed to different strains, then lightly annealed, and the crystallographic aspects of the recrystallization process along shear bands examined by local orientation measurement in TEM and SEM. The results clearly show the existence of a well-defined crystallographic relation between the local deformation substructure and the first recrystallized areas of uniform orientation. The first-formed nuclei always exhibit near 25–400(<111>–<112>) type misorientations, in the direction of highest growth, with respect to one of the two main groups of the deformation texture components. The rotation axes can be correlated with the slip plane normal of highest activity. As recrystallization proceeds, recrystallization twinning develops strongly and facilitates rapid growth; the first and higher generations of twins then tend to obscure the initial primary crystallographic relation between the shear bands and recrystallization nuclei .

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Authors and Affiliations

H. Paul
J.H. Driver
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Abstract

Abstract This paper assesses the effect of various values of detonation velocity on the quality of the bond zone, and thus the properties of bimetal zirconium (Zr 700) - steel (P355NL). The research was carried out for as-bonded welds, i.e. immediately following explosion welding. The results of shearing, peeling and tensile tests as well as macro-scale structural analyses were presented. In order to determine the changes in the value of strain hardening, the microhardness measurements across the interface were carried out. Based on the performed analyses it can be claimed that, depending on the applied technological settings of welding, most cases displayed wavy bond with highly diversified parameters of the wave. The changes observed with the detonation velocity are non-monotonic. High detonation velocities favored the formation of waves with large height and length and strongly affect the increase of the volume of brittle melted zones. Increased volume of the melted regions results in strong decrease of strength properties of the clad. The analysis of strength test results allows claiming that a small volume of melted regions in the bond considerably improves the strength of the bond.As a result of explosion welding, strain hardening of the joined materials occurs near the interface. In the case of clad fabricated using high technological parameters the increase of strengthening and the depth of its influence in the interface area is observed.
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Authors and Affiliations

M. Prażmowski
H. Paul
F. Żok
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Abstract

In this work, the effect of heat transfer during explosive welding (EXW) and post-processing annealing on the microstructural and chemical composition changes have been thoroughly analysed using scanning and transmission electron microscopies and X-ray synchrotron radiation. Several combination of explosively welded metal compositions were studied: Ti with Al, Cu with Al, Ta or stainless steel, stainless steel with Zr or Ta and Ti with carbon steel. It was found that the melted metals exhibit a strong tendency to form brittle crystalline, nano-grained or even amorphous phases during the solidification. For all analysed metal combinations most of the phases formed in the zones of solidified melt do not appear in the equilibrium phase diagrams. Concurrently, the interfacial layers undergo severe plastic deformation forming nano-grained structures. It has been established that these heavily deformed areas can undergo dynamic recovery and recrystallization already during clad processing. This leads to the formation of new stress-free grains near the interface. In the case of low temperature and short time post processing annealing only the melted zones and severely deformed layers undergo recovery and recrystallization. However, drastic changes in the microstructure occurs at higher temperature and for longer annealing times. Applying such conditions leads to diffusion dominant processes across the interface. As a consequence continuous layers of intermetallic phases of equilibrium composition are obtained.

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Authors and Affiliations

H. Paul
M.M. Miszczyk
A. Gałka
R. Chulist
Z. Szulc
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Abstract

Development of a reliable numerical model capturing major physical mechanisms controlling explosive welding and considering properties of all process components i.e. base plate and flyer plate is the goal of the paper. To properly replicate materials behavior under these severe conditions a meshfree approach, namely Smooth Particle Hydrodynamics (SPH), was used to discretize the computational domain. The model is based on the Mie-Gruneisen shock equation of state applied to the Ti/Cu system as a case study. Examples of results in the form of velocity, equivalent stress, equivalent strain, and pressure fields are presented within the paper.

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Authors and Affiliations

M. Mojżeszko
K. Perzyński
M. Sionkowski
H. Paul
ORCID: ORCID
Ł. Madej
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Abstract

Multilayered composites based on light metals are promising materials in many applications. In the present work the 15-layered clad, composed of alternately stacked of Ti(Gr.1) and AA1050-H24 alloy sheets of 1 mm thick has been investigated with respect to determination of the kinetic of the Al3Ti phase growth. The defect-free multilayered composite was successfully formed by explosive welding technology. Then EXW samples were modified via annealing at the temperature of 600oC in closed die under pressure of 44 MPa for various times ranged between 1 and 10 h. Transmission and Scanning Electron Microscopy examinations were conducted in order to study the kinetic of the elements migration across the interfaces between the layers of the Al/Ti composite. The macro-scale observations of samples after EXW revealed that wavy interfaces were always formed in layers near the explosive charge. The increase of the distance from the top surface leads to flattening of the interface with very thin reaction layer between Al and Ti sheets. During annealing the kinetic of the Al3Ti phase growth is similar near all interfaces and coincides with data from other works. It was found that despite the loading after 10 h of annealing still only small part of Al-sheets undergoes dissolution and the width of the reaction layer does not exceed 5-8 µm.

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Authors and Affiliations

P. Petrzak
ORCID: ORCID
I. Mania
ORCID: ORCID
H. Paul
ORCID: ORCID
Ł. Maj
ORCID: ORCID
A. Gałka
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Abstract

In this paper, the microstructural and texture changes in polycrystalline CuZn30 alloy, copper, and AA1050 aluminium alloy have been studied to describe the crystal lattice rotation during shear bands formation. The hat-shaped specimens were deformed using a drop-hammer at the strain rate of 560 s –1. Microstructure evolution was investigated using optical microscopy, whereas texture changes were examined with the use of a scanning electron microscope equipped with the EBSD facility. The microstructural observations were correlated with nanohardness measurements to evaluate the mechanical properties of the sheared regions. The analyses demonstrate the gradual nature of the shear banding process, which can be described as a mechanism of the bands nucleation and then successive growth rather than as an abrupt instability. It was found that regardless of the initial orientation of the grains inside the sheared region, a well-defined tendency of the crystal lattice rotation is observed. This rotation mechanism leads to the formation of specific texture components of the sheared region, different from the one observed in a weakly or non-deformed matrix. During the process of rotation, one of the {111} planes in each grain of the sheared region ‘tends’ to overlap with the plane of maximum shear stresses and one of the <110> or <112> directions align with the shear direction. This allows slip propagation through the boundaries between adjacent grains without apparent change in the shear direction. Finally, in order to trace the rotation path, transforming the matrix texture components into shear band, rotation axis and angles were identified.
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Authors and Affiliations

I. Mania
1
ORCID: ORCID
H. Paul
1
ORCID: ORCID
R. Chulist
1
ORCID: ORCID
P. Petrzak
1
ORCID: ORCID
M. Miszczyk
1
ORCID: ORCID
M. Prażmowski
2
ORCID: ORCID

  1. Polish Academy of Sciences, Institute of Metallurgy and Materials Science, 25 Reymonta Str., 30-059 Krakow, Poland
  2. Opole University of Technology, Faculty of Mechanics, 76 Prószkowska Str., 45-758 Opole, Poland
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Abstract

Metal-intermetallic layered (MIL) composites attract considerable attention due to their remarkable structural and ballistic performance. This study aimed to develop a Ti/Al-based multilayered MIL material by adding ceramic powders, since they can improve the composite’s impact resistance. To this end, an experiment was conducted which a stack of alternating Ti and Al sheets bonded by hot pressing; Ti/Al multilayers containing additional layers of Al2O3 and SiC powders were also produced. The samples obtained were examined using electron microscopy techniques. The clads’ mechanical properties were investigated using a Charpy hammer. In the reaction zone, only one intermetallic phase occurred: the Al3Ti phase. The model with an additional Al2O3 layer showed the highest impact energy. None of the Ti/Al clads broke during the Charpy impact test, a result proving their high ductility.
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Bibliography

[1] I.A. Bataev, A.A. Bataev, V.I. Mali, D.V. Pavliukova, Structural and mechanical properties of metallic-intermetallic laminate composites produced by explosive welding and annealing, Mater. Design 35, 225-234 (2012). DOI: https://doi.org/10.1016/j.matdes.2011.09.030
[2] F. Foadian, M. Soltanieh, M. Adeli, M. Etminanbakhsh, A Study on the Formation of Intermetallics During the Heat Treatment of Explosively Welded Al-Ti Mulitlayers, Metall. Mater. Trans. A 45A, 1823 (2014). DOI: https://doi.org/10.1007/s11661-013-2144-6
[3] H. Paul, Ł. Maj, M. Prażmowski, A. Gałka, M. Miszczyk, P. Petrzak, Microstructure and mechanical properties of multilayered Al/Ti composites produced by explosive welding, Procedia Manufacturing 15, 1391-1398 (2018). DOI: https://doi.org/10.1016/j.promfg.2018.07.343
[4] D.M. Fronczek, R. Chulist, Z. Szulc, J. Wojewoda-Budka, Growth kinetics of TiAl3 phase in annealed Al/Ti/Al explosively welded clads, Mater. Lett. 198, 160-163 (2017). DOI: https://doi.org/10.1016/j.matlet.2017.04.025
[5] F. Kong, Y. Chen, D. Zhang, Interfacial microstructure and shear strength of Ti-6Al-4V/TiAl laminate composite sheet fabricated by hot packed rolling, Mater. Design 32, 3167-3172 (2011). DOI: https://doi.org/10.1016/j.matdes.2011.02.052
[6] H. Xiao, Z. Qi, C. Yu, C. Xu, Preparation and properties for Ti/ Al clad plates generated by differential temperature rolling, J. Mater. Process. Tech. 249, 285-290 (2017). DOI: https://doi.org/10.1016/j.jmatprotec.2017.06.013
[7] M. Fan, Z. Luo, Z. Fu, X. Guo, J. Tao, Vacuum hot pressing and fatigue behaviors of Ti/Al laminate composites, Vacuum 154, 101- 109 (2018). DOI: https://doi.org/10.1016/j.vacuum.2018.04.047
[8] L. Qin, M. Fan, X. Guo, J. Tao, Plastic deformation behaviors of Ti-Al laminated composite fabricated by vacuum hot-pressing, Vacuum 155, 96-107 (2018). DOI: https://doi.org/10.1016/j.vacuum.2018.05.021
[9] J . Li, K.H. Wang, K. Zhang L.L. Kang, H. Liang, Mechanism of interfacial reaction between Ti and Al-ceramic, Mater. Design 105, 223-233 (2016). DOI: https://doi.org/10.1016/j.matdes.2016.05.073
[10] G .H.S.F.L. Carvalho, I. Galvão, R. Mendes, R.M. Leal, A. Loureiro, Explosive welding of aluminium to stainless steel, J. Mat. Process. Tech. 262, 340-349 (2018). DOI: https://doi.org/10.1016/j.jmatprotec.2018.06.042
[11] I. D. Zakharenko, Critical conditions in detonation welding, Fizika Goreniya i Vzryva 8 (3), 422-427 (1972).
[12] M. Tayyebi, D. Rahmatabadi, M. Adhami, R. Hashemi, Influence of AR B technique on the microstructural, mechanical and fracture properties of the multilayered Al1050/Al5052 composite reinforced by SiC particles, J. Mater. Res. Tech. 8 (5), 4287-4301 (2019). DOI: https://doi.org/10.1016/j.jmrt.2019.07.039
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Authors and Affiliations

W. Kowalski
1
ORCID: ORCID
H. Paul
1
ORCID: ORCID
P. Petrzak
1
ORCID: ORCID
Ł. Maj
1
ORCID: ORCID
I. Mania
1
ORCID: ORCID
M. Faryna
1
ORCID: ORCID

  1. Institute of Metallurgy and Materials Science , Polish Academy of Sciences , 25 Reymonta Str., 30-059 Kraków, Poland
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Abstract

This study aimed to develop Fe/Al multilayered metallic/intermetallic composites produced by hot pressing under an air atmosphere. Analyses were carried out on the composite plates made up of alternatively situated sheets of AA1050 aluminum alloy and DN04 low carbon steel, which were annealed at 903 K for 2, 5, and 10 h. Annealing was performed to obtain reaction layers of distinct thickness. The samples were examined using X-Ray diffraction and scanning and transmission electron microscope equipped with an energy-dispersive X-Ray spectrometer. To correlate the structural changes with mechanical properties, microhardness measurements in near-the-interface layers were performed. All the reaction layers grew with parabolic kinetics with η-Al5Fe2 intermetallic phase as the dominant component. After annealing for 5 and 10 hours, a thin sublayer of θ-Al13Fe4 phase was also detected.
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Authors and Affiliations

W. Kowalski
1
ORCID: ORCID
H. Paul
1
ORCID: ORCID
I. Mania
1
ORCID: ORCID
P. Petrzak
1
ORCID: ORCID
P. Czaja
1
ORCID: ORCID
R. Chulist
1
ORCID: ORCID
A. Góral
1
ORCID: ORCID
M. Szlezynger
1
ORCID: ORCID

  1. Institute of Metallurgy and Materials Science, Polish Academy of Sciences, 25 Reymonta Str., 30-059 Krakow, Poland

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