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Abstract

Generally, the metallic implants do not exhibit any bio-integration properties in contact with bone tissues. To improve the interfacial properties of metallic implants in contact with bone, the coatings with thin biocompatible films are used. Two methods to coating titanium implants with hydroxyapatite are described. The first is a two phase method, where by cathodic polarization is deposed a monetite film followed by an alkaline treatment when the monetite is converted to hydroxyapatite. The second method is a biomimetic deposition on an alkaline activate titanium surface, using a five time more concentrated simulated body fluid (5xSBF). After deposition this samples was drying at 120℃ and was sintered at 700℃ for three hours. Optical microscopy, Fourier Transform Infrared Spectroscopy (FTIR), Scanning Electron Microscopy (SEM) and Energy-dispersive X-ray (EDX) were used to characterize structure, morphology and compositions of the deposed films. In this study, electrochemical deposition and biomimetic deposition of hydroxyapatite are compared.
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Authors and Affiliations

M.C. Perju
1 2 3
ORCID: ORCID
C. Nejneru
1
ORCID: ORCID
P. Vizureanu
1 2 3
ORCID: ORCID
A.A. Aelenei
1
ORCID: ORCID
A.V. Sandu
1 2 3
ORCID: ORCID
L. Sachelarie
4
ORCID: ORCID
M. Nabiałek
5
ORCID: ORCID

  1. "Gheorghe Asachi” Technical University of Iasi, Faculty of Materials Science and Engineering, Prof. D. Mangeron Street, No. 41, 700050, Iasi, Romania
  2. Universiti Malaysia Perlis (UniMAP), Centre of Excellence Geopolymer and Green Technology (CEGeoGTech ), Perlis, Malaysia
  3. Romanian Inventors Forum, Sf. P. Movila 3, Iasi, Romania
  4. Apollonia University of Iasi, Faculty of Dentistry, PACURARI STREET, NO. 11, 700511, Iasi, Romania
  5. Częstochowa University of Technology, Department of Physics , 42-200 Częstochowa, Poland
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Abstract

Quenching technology requires the use of media with different cooling intensities and various shapes of cooling curves that show different particularities compared to that of conventional media such as water, oil, or emulsions. The use of synthetic quenching media is relatively new and also has multiple advantages such as non-flammability, safety in use and low cost. In this study, the cooling media tested was obtained by mixing 2 wt% carboxymethyl cellulose with 2 wt% NaOH in one litter of water. Moreover, three different temperatures (20°C, 40°C and 60°C) of the quenching media were evaluated. By dissolution in water, a synthetic solution with low viscosity, surfactant and lubricant was obtained. Because carboxymethyl cellulose is a biodegradable organic material, that is obtained as a by-product in the manufacture of paper, a basic substance with a preservative effect was added. According to this study, both the variation diagram of the heat transfer coefficient and the diagram of the cooling rates, during the cooling stages give important indications regarding the use of a liquid cooling medium for quenching.
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Authors and Affiliations

M.C. Perju
1
ORCID: ORCID
C. Nejneru
1
ORCID: ORCID
D.D. Burduhos-Nergis
1 2
ORCID: ORCID
P. Vizureanu
1 2
ORCID: ORCID
M.G. Minciuna
1
ORCID: ORCID
A.V. Sandu
1 2
ORCID: ORCID

  1. “Gheorghe Asachi” Technical University of Iasi, Faculty of Materials Science and Engineering, Prof. D. Mangeron Street, No. 41, 700050, Iasi, Romania
  2. Romanian Inventors Forum, Sf. P. Movila 3, Iasi, Romania

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