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Number of results: 13
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Abstract

The aim of the performed experiments was to determine the influence of a cooling rate on the evolution of microstructure and hardness of the steel 27MnCrB5. By using dilatometric tests performed on the plastometer Gleeble 3800 and by using mathematical modelling in the software QTSteel a continuous cooling transformation diagram for a heating temperature of 850°C was constructed. Conformity of diagrams constructed for both methods is relatively good, except for the position and shape of the ferrite nose. The values of hardness, temperatures of phase transformations and the volume fractions of structural phases upon cooling from the temperature of 850°C at the rate from 0.16°C · s–1 to 37.2°C · s–1 were determined. Mathematically predicted proportion of martensite with real data was of relatively solid conformity, but the hardness values evaluated by mathematical modelling was always higher.
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Authors and Affiliations

I. Schindler
P. Kawulok
J. Mizera
S. Rusz
R. Kawulok
P. Opěla
M. Olszar
K.M. Čmiel
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Abstract

The study attempts to investigate the influence of severe plastic deformation (SPD in the hydrostatic extrusion (HE) process on the anisotropy of the structure and mechanical properties of the AA 6060 alloy. Material in isotropic condition was subjected to a single round of hydrostatic extrusion with three different degrees of deformation (ε  = 1.23, 1.57, 2.28). They allowed the grain size to be fragmented to the nanocrystalline level. Mechanical properties of the AA 6060 alloy, examined on mini-samples, showed an increase in ultimate tensile strength (UTS) and yield strength (YS) as compared to the initial material. Significant strengthening of the material results from high grain refinement in transverse section, from »220 μm in the initial material to »300 nm following the HE process. The material was characterized by the occurrence of structure anisotropy, which may determine the potential use of the material. Static tensile tests of mini-samples showed »10% anisotropy of properties between longitudinal and transverse cross-sections. In the AA6060 alloy, impact anisotropy was found depending on the direction of its testing. Higher impact toughness was observed in the cross-section parallel to the HE direction. The results obtained allow to analyze the characteristic structure created during the HE process and result in more efficient use of the AA 6060 alloy in applications.

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Authors and Affiliations

S. Przybysz
M. Kulczyk
W. Pachla
J. Skiba
M. Wróblewska
J. Mizera
D. Moszczyńska
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Abstract

The aim of the present work was to determine the influence of the microstructural evolution of copper single crystals with the initial orientations of <001> and <111> after cold drawing on their corrosion resistance. Transmission electron microscopy, X-ray diffraction, and electron backscattering diffraction were used to characterize the microstructural changes. To evaluate the corrosion resistance after deformation, open circuit potential, electrochemical impedance spectroscopy, and potentiodynamic polarization analyses were conducted. The microstructural observations showed the presence of dislocation cell structures and shear bands in deformed sample with initial orientation <001> single crystal, as well as a strongly-developed substructure in sample <111>. The material with initial orientation of <001> was more resistive in analyzed medium than material with the initial orientation of <111>.

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Authors and Affiliations

M. Koralnik
A. Dobkowska
B. Adamczyk-Cieślak
ORCID: ORCID
J. Mizera
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Abstract

The paper presents the results of the electrodeposition of nickel composite coatings reinforced with the ceramic SiC particles. A Watts type galvanic bath modified with various organic additives was used. These additives were: 2-sulfobenzoic acid imide (LSA), dioctyl sulfosuccinate sodium salt (DSS), sodium dodecyl sulfate (SDS), tris (hydroxymethyl) aminomethane (THAM) and hexamethyldisilizane (HMDS). The nickel composite coating was electrodeposited on a 2xxx aluminum alloy series substrate (EN-AW 2017) with zinc interlayer. Studies concerned the effect of the applied organic additives on properties of composite coatings such as: microstructure, microhardness, adhesion to the substrate, corrosion resistance and roughness. The structure of the coatings was assessed by scanning electron microscopy and light microscopy. Based on the studies of zeta potential it was found that the bath modification had a significant impact on the amount of the ceramic phase embedded in metal matrix. The tests conducted in a model 0.01 M KCl solution were not fully representative of the true behavior of particles in a Watts bath.

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Authors and Affiliations

M. Nowak
J. Mizera
A. Kłyszewski
A. Dobkowska
S. Boczkal
ORCID: ORCID
A. Kozik
P. Koprowski
ORCID: ORCID
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Abstract

The paper presents the results of the electrodeposition of nickel composite coatings reinforced with the nano size SiC ceramic particles. The type and size of the ceramic particles or organic additives used play a important role during electrodeposition processes. A Watts type galvanic bath with various organic additives was used. These additives were: 2-sulfobenzoic acid imide, dioctyl sulfosuccinate sodium salt (DSS), sodium dodecyl sulfate, tris (hydroxymethyl) aminomethane and hexamethyldisilizane. The nickel composite coating was electrodeposited on a 2xxx aluminum alloy series substrate (EN-AW 2017) with zinc interlayer. The work concerns the determination of the impact of the change in the zeta potential of SiC nanoceramic particles used on properties of composite coatings (wear resistance, corrosion, etc.). The paper characterized the composite nickel coatings on aluminum alloy using SEM techniques, wear resistance tests by TABER method and coating adhesion to the substrate using the “scratch test” method. The corrosion resistance of coatings was also tested using electrochemical methods. The research allowed to determine the effect of SiC nanoceramic particle size on the value of the zeta potential in the model KCl solution.

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Authors and Affiliations

M. Nowak
J. Mizera
A. Kłyszewski
A. Dobkowska
S. Boczkal
ORCID: ORCID
A. Kozik
P. Koprowski
ORCID: ORCID

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