@ARTICLE{Kim_B.-W._Fabrication_2018, author={Kim, B.-W. and Huynh, X.-K. and Kim, J.-S.}, volume={vol. 63}, number={No 2}, journal={Archives of Metallurgy and Materials}, howpublished={online}, year={2018}, publisher={Institute of Metallurgy and Materials Science of Polish Academy of Sciences}, publisher={Committee of Materials Engineering and Metallurgy of Polish Academy of Sciences}, abstract={Fe-40wt% TiB2 nanocomposites were fabricated by mechanical activation and spark-plasma sintering of a powder mixture of iron boride (FeB) and titanium hydride (TiH2). The powder mixture of (FeB, TiH2) was prepared by high-energy ball milling in a planetary ball mill at 700 rpm for 3 h followed by spark-plasma sintering (SPS) at various conditions. Analysis of the change in relative sintered density and densification rate during sintering showed that a self-propagating high-temperature synthesis reaction occurs to form TiB2 from FeB and Ti. A sintered body with relative density higher than 98% was obtained after sintering at 1150°C for 5 and 15 min. The microstructural observation of sintered compacts with the use of FE-SEM and TEM revealed that ultrafine particulates with approximately 5 nm were evenly distributed in an Fe-matrix. A hardness value of 83 HRC was obtained, which is equivalent to that of conventional WC-20 Co systems.}, type={Artykuły / Articles}, title={Fabrication of Fe-TiB2 Nanocomposites by Spark-Plasma Sintering of a (FeB, TiH2) Powder Mixture}, URL={http://www.czasopisma.pan.pl/Content/106720/PDF/AMM-2018-2-66-Kim.pdf}, doi={10.24425/122440}, keywords={Fe-TiB2 nanocomposite, mechanical activation, spark-plasma sintering, self-propagating high-temperature synthesis reaction}, }